The enclosed data are NMR spectroscopic data in mnova format (Maestre Nova v10) and mass spectral data in trans format for the compounds prepared in the paper "Cavity-Containing Supramolecular Gels as a Crystallization Tool for Hydrophobic Pharmaceuticals". 
Crystallographic data are deposited with the CCDC except the enclosed files for calixarene 2b which is of poor precision.